产品说明
应用
Screening kit for ring closing metathesis. Step-by-step user guides and a downloadable experimental excel sheets are provided in the below hyperlinks.
Step-by-Step Guide for Ring Closing Metathesis/Cross Metathesis Reaction Screening Kit Downloadable Experiment excel sheets
Each kit contains 2 customizable screening sets that include the following components:
- 6x4 pre-weighed catalysts in glass microvials loaded with stir bars and topped with cap mat.
- 2 (2 mL) ampules each of of ClPh, PhMe, i-PrOAc, Me-THF, and TFA.
- 1 KitAlysis 24-well reaction block replacement film.
- 4 empty substrate stock solution reaction vials with stir bars.
- 1 internal standard.
Best when used with KitAlysis Benchtop Inertion Box and 24-well Reaction Block (sold separately).
特点和优势
- Designed and tested by synthetic chemists.
- Easily run 24-microscale reaction in parallel.
- 20 μmol reactions with 1 μmol catalyst (5 mol%), 0.2 M concentration, and optional TFA additive.
- Customizable and downloadable excel template for quick calculations and easy incorporation into electronic laboratory notebooks.
法律信息
KitAlysis is a trademark of sigma-aldrich Co. LLC
产品性质
reaction suitability | core: palladium reaction type: Buchwald-Hartwig Cross Coupling Reaction reaction type: Heck Reaction reaction type: Hiyama Coupling reaction type: Negishi Coupling reaction type: Sonogashira Coupling reaction type: Stille Coupling reaction type: Suzuki-Miyaura Coupling reagent type: catalyst reaction type: Cross Couplings |
储存温度 | 2-8℃ |
组份列表
组份可单独销售
货号 | 组份 |
569747 | Grubbs Catalyst® M204, Umicore 3 µmol |
569755 | Hoveyda-Grubbs Catalyst® M720, Umicore, 97% 3 µmol |
579726 | Grubbs Catalyst® M102, Umicore, 97% 3 µmol |
682365 | Grubbs Catalyst® M207, Umicore 3 µmol |
682373 | Hoveyda-Grubbs Catalyst® M721, Umicore 3 µmol |
729345 | Hoveyda-Grubbs Catalyst® M722, Umicore 3 µmol |
900519 | Isopropyl acetate, anhydrous, ZerO2®, ≥99.6% 8 mL |
900520 | 2-Methyltetrahydrofuran, anhydrous, contains 250 ppm BHT as stabilizer, ZerO2®, ≥99.0% 8 mL |
900521 | Chlorobenzene, anhydrous, ZerO2®, 99.8% 8 mL |
900522 | Toluene, anhydrous, ZerO2®, 99.8% 8 mL |
Z118850 | Spinbar® magnetic stirring fleas, red, L 10 mm, diam. 3 mm 1 EA |
SnapIT Ampule Opener, Regular, for 1-2ml, 5-10ml, 10-15ml ampoules 1 EA |
安全信息
象形图 | |
警示用语: | Danger |
危险声明 | H228 - H302 + H332 - H315 - H318 - H336 - H361d - H373 - H411 |
预防措施声明 | P210 - P273 - P280 - P304 + P340 + P312 - P305 + P351 + P338 - P308 + P313 |
危险分类 | Acute Tox. 4 Inhalation - Acute Tox. 4 Oral - Aquatic Chronic 2 - Eye Dam. 1 - Flam. Sol. 2 - Repr. 2 - Skin Irrit. 2 - STOT RE 2 - STOT SE 3 |
靶器官 | Central nervous system |
补充剂危害 | EUH019 |
储存分类代码 | 4.1B - Flammable solid hazardous materials |
WGK | WGK 3 |