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KitAlysisTM High-Throughput Miyaura Borylation Reaction Screening Kit-Pack of 2

KitAlysisTM 高通量Miyaura硼化反应筛选试剂盒-2套

品牌
Sigma-Aldrich
货号
KITALYSIS-BOR
包装型号
规格纯度
参考价格
13844.9 *本价格含增值税费
促销
数量
-+
产品介绍:

产品说明

应用

Screening kit for Miyaura borylation reaction. Step-by-step user guides and a downloadable experimental excel sheets are provided in the below hyperlinks.
Step-by-Step Guide for Miyaura Borylation Reaction Screening Kit
Downloadable Experiment excel sheets

Each kit contains 2 customizable screening sets that include the following components:

  • 6 x 4 pre-weighed catalysts in glass vials loaded with stir bars and topped with cap mat.
  • 4 x 4 mL reaction vials with pre-weighed KOAc
  • Bis(pinacolato)diboron (473294), tetrahydroxydiboron (754242), and pinacol (221171)
  • 1 (2 mL) ampule each of toluene, THF, n-butanol, DMA, MeOH, MeCN, ethylene glycol and DIPEA.
  • 1 NEW KitAlysis 24-Well Reaction Block Replacement Film.
  • 4 stir bars for substrate stock solution vials.
  • 1 internal standard.

Best when used with KitAlysis Benchtop Inertion Box and 24-well Reaction Block (sold separately).

特点和优势

  • Designed and tested by synthetic chemists.
  • Easily run 24-microscale reactions in parallel.
  • 10 μmol reactions with 1 μmol catalyst, 3 equiv. base, 0.1 M concentration.
  • Customizable Excel Template for quick calculations and easy incorporation into electronic laboratory notebooks.

法律信息

KitAlysis is a trademark of sigma-aldrich Co. LLC

产品性质

reaction suitabilityreaction type: Buchwald-Hartwig Cross Coupling Reaction
reaction type: Cross Couplings
reaction type: Heck Reaction
reaction type: Hiyama Coupling
reaction type: Negishi Coupling
reaction type: Sonogashira Coupling
reaction type: Stille Coupling
reaction type: Suzuki-Miyaura Coupling
reagent type: catalyst
core: palladium
官能团phosphine

组份列表

组份可单独销售

货号组份
764175P(Cy3) Pd G3, 97%
791733Potassium acetate, anhydrous, free-flowing, Redi-Dri, ACS reagent, ≥99.0%
804274XPhos Pd G4, 95%
804282SPhos Pd G4
804290RuPhos Pd G4
804975DTBPF-Pd-G3
900349cataCXium Pd G4
900522Toluene, anhydrous, ZerO2®, 99.8%
900631Ethylene glycol, anhydrous, ZerO2®, 99.8%
900634N,N-Dimethylacetamide, anhydrous, ZerO2®, 99.8%
900636Tetrahydrofuran, anhydrous, inhibitor-free, ZerO2®, ≥99.9%
9006391-Butanol, anhydrous, ZerO2®, 99.8%
900641Methanol, anhydrous, ZerO2®, 99.8%
900644Acetonitrile, anhydrous, ZerO2®, 99.8%
900690N,N-Diisopropylethylamine, purified by redistillation, ZerO2®, 99.5%
221171Pinacol, 98%
473294Bis(pinacolato)diboron, 99%
754242Tetrahydroxydiboron, 95%
B34656Biphenyl, ReagentPlus®, 99.5%
Z118850Spinbar® magnetic stirring fleas, red, L 10 mm, diam. 3 mm
Z742110KitAlysis 24-well reaction block replacement film

安全信息

象形图GHS02GHS05GHS06GHS08GHS09
警示用语:Danger
危险声明H225 - H301 + H311 + H331 - H315 - H318 - H335 - H336 - H351 - H360D - H370 - H373 - H410
预防措施声明P210 - P273 - P280 - P301 + P310 - P303 + P361 + P353 - P305 + P351 + P338
危险分类Acute Tox. 3 Dermal - Acute Tox. 3 Inhalation - Acute Tox. 3 Oral - Aquatic Acute 1 - Aquatic Chronic 1 - Carc. 2 - Eye Dam. 1 - Flam. Liq. 2 - Repr. 1B - Skin Irrit. 2 - STOT RE 2 Oral - STOT SE 1
靶器官Kidney
补充剂危害EUH019
储存分类代码3 - Flammable liquids
WGKWGK 3
闪点(F)1.4 °F
闪点(C)-17 ℃

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